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Beilstein J. Org. Chem. 2015, 11, 2476–2486, doi:10.3762/bjoc.11.269
Graphical Abstract
Figure 1: General depictions of allyl and related precatalysts that are highly active for the Suzuki–Miyaura ...
Scheme 1: Synthesis of Cp.
Figure 2: Comparison of catalytic performance of Cin, Cp and tBuInd for a series of Suzuki–Miyaura reactions ...
Figure 3: Comparison of catalytic performance of Cin, Cp and tBuInd for a series of Suzuki–Miyaura reactions ...
Scheme 2: Proposed mechanism for the activation of Cp to monoligated Pd(0).
Scheme 3: Synthesis of CpDim.
Figure 4: ORTEP of CpDim at 30% probability. Hydrogen atoms and isopropyl groups of IPr are omitted for clari...
Scheme 4: Observation of CpDim under modified catalytic conditions.
Scheme 5: CpDim is not an active precatalyst for a Suzuki–Miyaura reaction at room temperature.
Scheme 6: Disproportionation of CpDim with dvds.
Scheme 7: a) Crossover experiment between Cp and (μ-allyl)(μ-Cl)Pd2(IPr)2. b) Crossover experiment expressed ...